𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Ethyl 4,6-dimethyl-2-thioxo-1,2,3,4-tetrahydro­pyrimidine-5-carboxyl­ate

✍ Scribed by Zavodnik, Valery E. ;Shutalev, Anatoly D. ;Gurskaya, Galina V. ;Stash, Adam I. ;Tsirelson, Vladimir G.

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
269 KB
Volume
61
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

Single-crystal X-ray study T = 292 K Mean '(C±C) = 0.002 A Ê R factor = 0.030 wR factor = 0.095 Data-to-parameter ratio = 14.9

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

Ethyl 5,5′′-dimethyl-2,2′;6′,2′′-terpyri
Ethyl 5,5′′-dimethyl-2,2′;6′,2′′-terpyridine-4′-carboxyl­ate
✍ Kickelbick, Guido ;Hoogenboom, Richard ;Schubert, Ulrich S. 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 296 KB

The title compound, C 20 H 19 N 3 O 2 , was synthesized by Stille coupling of ethyl 2,6-dibromoisonicotinate and 2-trimethylstannyl-5-methylpyridine. The three pyridine rings in the molecule are coplanar and the crystal packing revealsstacking interactions between these conjugated aromatic rings wit

Ethyl 4-(4-hydroxy­phenyl)-6-methyl-2-ox
Ethyl 4-(4-hydroxy­phenyl)-6-methyl-2-oxo-1,2,3,4-tetra­hydro­pyrimidine-5-carboxyl­ate
✍ Li, Ming ;Guo, Wei-Si ;Wen, Li-Rong ;Qi, Wen-Ying 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 150 KB

Single-crystal X-ray study T = 293 K Mean (C±C) = 0.003 A Ê Disorder in main residue R factor = 0.043 wR factor = 0.134 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.