Ethyl 3,5-bis(allyloxy)-4-bromobenzoate
✍ Scribed by Kirsop, Peter ;Storey, John M. D. ;Harrison, William T. A.
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 360 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The asymmetric molecular conformation of the title compound, C 15 H 17 BrO 4 , may be be influenced by an intramolecular C-HÁ Á ÁO interaction. The molecules formstacks in the crystal structure.
📜 SIMILAR VOLUMES
Dimethoxy-2,3-dimethylbenzene was brominated under radical conditions to give the title compound, C 10 H 11 Br 3 O 4 . The bond lengths and angles are generally within the normal ranges. The crystal packing is stabilized by weak intermolecular C-HÁ Á ÁO and C-HÁ Á ÁBr hydrogen bonds.
Single-crystal X-ray study T = 250 K Mean '(C±C) = 0.003 A Ê R factor = 0.044 wR factor = 0.125 Data-to-parameter ratio = 12.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.