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Ethyl 3,5-bis­(all­yloxy)-4-bromo­benzoate

✍ Scribed by Kirsop, Peter ;Storey, John M. D. ;Harrison, William T. A.


Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
360 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis


The asymmetric molecular conformation of the title compound, C 15 H 17 BrO 4 , may be be influenced by an intramolecular C-HÁ Á ÁO interaction. The molecules formstacks in the crystal structure.


📜 SIMILAR VOLUMES


1-Bromo-3,4-bis­(bromo­meth­yl)-2,5-dime
✍ Hammershøj, Peter ;Riis, Erik ;Christensen, Jørn B. 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 242 KB

Dimethoxy-2,3-dimethylbenzene was brominated under radical conditions to give the title compound, C 10 H 11 Br 3 O 4 . The bond lengths and angles are generally within the normal ranges. The crystal packing is stabilized by weak intermolecular C-HÁ Á ÁO and C-HÁ Á ÁBr hydrogen bonds.

2-(3,4-Di­methoxy­phenyl)­ethyl­ammonium
✍ Ohba, Shigeru ;Ito, Yoshikatsu 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 234 KB

Single-crystal X-ray study T = 250 K Mean '(C±C) = 0.003 A Ê R factor = 0.044 wR factor = 0.125 Data-to-parameter ratio = 12.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.