The title compound, C 22 H 19 NO 6 , was synthesized by the reaction of 4-hydroxycoumarin and ethyl 4 H -methoxy-2-cyanocinnamate in the presence of triethylbenzylammonium chloride in an aqueous medium. In the crystal structure, the amino group is involved in both intra-and intermolecular NÐ HÁ Á ÁO
Ethyl 2-amino-4-(4-methoxyphenyl)-7-methyl-5-oxopyrano[3,2-c]pyran-3-carboxylate
✍ Scribed by Shi, Da-Qing ;Niu, Li-Hui ;Wang, Xiang-Shan ;Zhuang, Qi-Ya ;Zhang, Yong
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 374 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.003 A Ê Disorder in main residue R factor = 0.040 wR factor = 0.101 Data-to-parameter ratio = 12.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê Disorder in solvent or counterion R factor = 0.054 wR factor = 0.170 Data-to-parameter ratio = 14.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.