Ethyl 2-amino-4-(4-chlorophenyl)-6-(4-methoxyphenyl)pyridine-3-carboxylate
✍ Scribed by Zhu, Yuezhao ;Tu, Shujiang ;Fang, Fang ;Xu, Jianing
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 213 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 193 K Mean '(C±C) = 0.002 A Ê R factor = 0.050 wR factor = 0.115 Data-to-parameter ratio = 16.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 292 K Mean '(C±C) = 0.004 A Ê R factor = 0.044 wR factor = 0.127 Data-to-parameter ratio = 12.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 23 H 21 NO 4 , was synthesized by the reaction of 1-naphthol with ethyl cyanocaetate and 4methoxybenzaldehyde in ethanol under microwave irradiation. In the structure of C 23 H 21 NO 4 , there are intramolecular and intermolecular N-HÁ Á ÁO hydrogen bonds, also C-HÁ Á Á interac
In the title compound, C 27 H 23 N 3 O 5 , the pyrimidine ring is slightly puckered. The mean plane of the pyrimidine ring forms dihedral angles of 28.26 (10), 55.53 (9) and 55.96 (10) with the three benzene rings in the molecule. There are intramolecular and intermolecular C-HÁ Á ÁO interactions.