Ethyl 2-[2,2-bis(ethoxycarbonyl)ethyl]-1-(phenylsulfonyl)indole-3-carboxylate

✍ Scribed by Chakkaravarthi, G. ;Dhayalan, V. ;Mohanakrishnan, A. K. ;Manivannan, V.

• Publisher: International Union of Crystallography
• Year: 2007
• Tongue: English
• Weight: 423 KB
• Volume: 63
• Category: Article
• ISSN: 1600-5368
• DOI: 10.1107/s1600536807057078

✦ Synopsis

Mo K radiation = 0.17 mm À1 T = 295 (2) K 0.26 Â 0.18 Â 0.14 mm

Data collection

Bruker Kappa APEX2 diffractometer Absorption correction: multi-scan (SADABS; Sheldrick, 1996) T min = 0.892, T max = 0.976 29408 measured reflections 6381 independent reflections 4267 reflections with I > 2(I) R int = 0.032 Refinement R[F 2 > 2(F 2 )] = 0.060 wR(F 2 ) = 0.192 S = 1.09 6381 reflections 356 parameters 10 restraints H-atom parameters constrained Á max = 0.38 e A ˚À3 Á min = À0.34 e A ˚À3

Table 1

Hydrogen-bond geometry (A ˚, ).