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Ethyl 2-[1-(ferrocenylcarbon­yl)prop-1-en-2-ylamino]-3-hydroxy­propionate dichloro­methane solvate

✍ Scribed by Shi, Yao-Cheng ;Sui, Chun-Xia ;Yang, Hua-Mei


Book ID
104485087
Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
144 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis


The title compound, [Fe(C 5 H 5 )(C 14 H 18 NO 4 )]ÁCH 2 Cl 2 , has been synthesized by the reaction of ferrocenoylacetone with dl-serine ethyl ester in ethanol. Electron delocalization is observed within the enaminone moiety.


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(2E)-3-(Biphenyl-4-yl)-1-(2,4-dichloro­p
✍ Fischer, Andreas ;Yathirajan, H. S. ;Ashalatha, B. V. ;Narayana, B. ;Sarojini, B 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 132 KB

The title compound, C~21~H~14~Cl~2~O, was prepared from biphenyl-4-carbaldehyde and 2,4-dichloroacetophenone. Single crystals were obtained from acetone. The compound crystallizes with four molecules in the asymmetric unit, all of which deviate significantly from planarity.