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Ethyl 1-benzoyl-4-chloro-2-phenylprolinate

✍ Scribed by Tamazyan, Rafael ;Ayvazyan, Armen ;Martirosyan, Ashot ;Martirosyan, Vahan ;Schinazi, Raymond

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
603 KB
Volume
63
Category
Article
ISSN
1600-5368

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In the title compound, C 22 H 16 ClN 3 O 3 , molecules are linked into chains along the c axis by C-HÁ Á ÁO hydrogen bonds, while other C-HÁ Á ÁN hydrogen bonds connect the chains into two-dimensional layers. The packing is further stabilized byinteractions.

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In the crystal structure of the title compound, C 22 H 16 ClN 3 O 3 , weak intermolecular C-HÁ Á ÁN hydrogen bonds link the molecules into chains extended along the c axis. The packing is further stabilized by weak C-HÁ Á ÁO interactions.

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The title compound, C 26 H 25 NO 3 , was synthesized by the 1,3dipolar cycloaddition reaction of benzaldehyde, -bromoacetophenone and N-benzylideneglycine ethyl ester. In the molecule, the heterocyclic five-membered ring adopts an envelope conformation.

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In the title compound, C 24 H 21 N 3 O 3 , the relative orientation of the three rings is determined by the sp 3 -hybridization character of the chiral atom. The molecules are linked into ribbons along the b axis by intermolecular C-HÁ Á ÁO interactions.