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Ethanolthermal synthesis to γ-CuI nanocrystals at low temperature

✍ Scribed by Yuanfang Liu; Jinhua Zhan; Jinghui Zeng; Yitai Qian; Kaibin Tang; Weichao Yu

Book ID
110317050
Publisher
Springer
Year
2001
Tongue
English
Weight
103 KB
Volume
20
Category
Article
ISSN
0261-8028

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Solvothermal Coordination–Reduction Rout
Solvothermal Coordination–Reduction Route to γ-NiSb Nanocrystals at Low Temperature
✍ Yi Xie; Jun Lu; Ping Yan; Xuchuan Jiang; Yitai Qian 📂 Article 📅 2000 🏛 Elsevier Science 🌐 English ⚖ 177 KB

A very mild synthesis of nanocrystalline -NiSb via a novel solvothermal coordination-reduction process is reported here. The reaction of the mixture of NiCl 2 , antimony, and KBH 4 was carried out in ethylenediamine (en) at 1403C for 24 h. X-ray powder di4raction and transmission electron microscope