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Ethanol­(ethoxy)[3-methoxy­salicyl­aldehyde (4-methoxy­benzoyl)­hydrazonato-κ3O,N,O′]­oxovanadium(V)

✍ Scribed by Huo, Li-Hua ;Gao, Shan ;Liu, Ji-Wei ;Zhao, Hui ;Ng, Seik Weng

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
185 KB
Volume
60
Category
Article
ISSN
1600-5368

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(Benzoyl­acetone 4-methoxy­benzoyl­hydra
(Benzoyl­acetone 4-methoxy­benzoyl­hydrazonato-κ3O,N,O′)(N-benzoyl­hydroxy­laminato-κ2O,O′)­oxovanadium(IV)
✍ Gao, Shan ;Huo, Li-Hua ;Zhao, Hui ;Ng, Seik Weng 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 181 KB

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê Disorder in main residue R factor = 0.036 wR factor = 0.110 Data-to-parameter ratio = 12.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

(N-Hydro­xy-N-phenyl­benzamidato-κ2O,O′)
(N-Hydro­xy-N-phenyl­benzamidato-κ2O,O′)[3-methoxy­salicyl­aldehyde (2,4-di­chlorophenoxy­acetyl)­hydrazonato-κ3O,N,O′]oxovanadium(V)
✍ Gao, Shan ;Liu, Ji-Wei ;Huo, Li-Hua ;Zhao, Hui 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 212 KB

The V V atom in the title complex, [V(C 16 H 12 C 12 N 2 O 4 )-(C 13 H 10 NO 2 )O], is coordinated by two O atoms and one N atom of the tridentate hydrazone ligand, and by two O atoms of the bidentate hydroxamate co-ligand, thus de®ning a distorted octahedral VO(ONO)(ON) geometry.