EPR spectra of products of the reaction of di-η5-cyclopentadienyl(diethylalanedi-μ-chloro)titanium(III) with C1 compounds
✍ Scribed by S.K. Tyrlik; A. Korda; L. Poppe; A. Rockenbauer; M. Györ
- Publisher
- Elsevier Science
- Year
- 1987
- Tongue
- English
- Weight
- 353 KB
- Volume
- 336
- Category
- Article
- ISSN
- 0022-328X
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📜 SIMILAR VOLUMES
The trichlorides of yttrium, samarium, and lutetium react with 2 equivalents of Na[C 5 H 4 t Bu] and 1 equivalent of NaBH 4 to give [(g 5 -C 5 H 4 t Bu) 2 LnBH 4 (THF)] (Ln = Y (1), Sm (2), Lu (3)) or with 2 equivalents of Na[C 5 Me 4 R] and 1 equivalent of NaBH 4 to form [(g 5 -C 5 Me 4 R) 2 ĹnBH 4
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê Disorder in solvent or counterion R factor = 0.047 wR factor = 0.137 Data-to-parameter ratio = 14.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.