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Enzymatic synthesis of [4R-2H]NAD(P)H and [4S-2H]NAD(P)H and determination of the stereospecificity of 7α- and 12α-hydroxysteroid dehydrogenase

✍ Scribed by Gianluca Ottolina; Sergio Riva; Giacomo Carrea; Bruno Danieli; Andreas F. Buckmann

Book ID
113267489
Publisher
Elsevier Science
Year
1989
Tongue
English
Weight
619 KB
Volume
998
Category
Article
ISSN
0167-4838

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The synthesis of 4-2H-α-farnesene and 1-
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✍ Simon Fielder; Daryl D. Rowan; Peter F. Reay 📂 Article 📅 1993 🏛 John Wiley and Sons 🌐 French ⚖ 580 KB

## Abstract α‐Farnesene deuterated at C1 or C4 was synthesised by regiospecific deuteration of 2‐geranyl‐3‐methylsulpholene (2). Treatment of (2) with butyl lithium in dimethylpropenylurea (DMPU) mediated THF resulted in deprotonation at C2. Quenching with D~2~O/CH~3~CO~2~D gave a mixture of deuter