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Enthalpie der Polymerisation von 7-Oxabicyclo[2.2.1]-heptan sowie exo- und endo-2-Methyl-7-oxabicyclo-[2.2.1]-heptan

✍ Scribed by F. Andruzzi; G. Pilcher; Y. Virmani; P. H. Plesch

Publisher
Springer
Year
1978
Weight
172 KB
Volume
256
Category
Article
ISSN
0340-255X

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## Abstract The polymerization of exo‐2‐methyl‐7‐oxabicyclo[2, 2, 1] heptane by PF 5 in ethylene dichloride solution was investigated. The reaction was followed in vacuum dilatometers fitted with platinum wire electrodes, which allowed us to measure the variations of conductivity during the polymer

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a Values are for individual samples. During the test, one could observe particles of the disintegrated tablet forming a ring at the bottom of the fabricated flask (Fig. 3). It is not likely that one would use the type of dissolution vessel shown in Fig. 2 when the other two types are commercially