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Enhanced microwave-assisted method for on-bead disulfide bond formation: Synthesis of α-conotoxin MII

✍ Scribed by Athanassios S. Galanis; Fernando Albericio; Morten Grøtli


Book ID
101718624
Publisher
Wiley (John Wiley & Sons)
Year
2009
Tongue
English
Weight
465 KB
Volume
92
Category
Article
ISSN
0006-3525

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A method for the one-pot regioselective
✍ Alan Cuthbertson; Bård Indrevoll 📂 Article 📅 2000 🏛 Elsevier Science 🌐 French ⚖ 78 KB

A one-pot method for the regioselective formation of the disulfide bridges of α-conotoxin SI employing temperature-controlled orthogonal protecting groups is reported. The pairing of t-butyl and 4-methylbenzyl sidechain protecting groups was chosen for the four cysteine residues. Cleavage of the pep