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Enhanced chromatographic NMR with polyethyleneglycol. A novel resolving agent for diffusion ordered spectroscopy

✍ Scribed by Jari S. Kavakka; Viktor Parviainen; Kristiina Wähälä; Ilkka Kilpeläinen; Sami Heikkinen


Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
228 KB
Volume
48
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

NMR analysis of complex mixtures can be significantly simplified using polyethyleneglycol (PEG) as resolving additive in DOSY NMR technique, which allows the extraction of individual spectra of mixture components with differing polarity. Resolving power of PEG‐assisted DOSY was demonstrated with natural product mixtures. Copyright © 2010 John Wiley & Sons, Ltd.