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Enantioselective Total Synthesis of (+)-(2 R ,6 R )- trans -γ-Irone

✍ Scribed by Monti, Honoré; Audran, Gérard; Monti, Jean-Pierre; Leandri, Gilbert

Book ID
126042450
Publisher
American Chemical Society
Year
1996
Tongue
English
Weight
156 KB
Volume
61
Category
Article
ISSN
0022-3263

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Cyclobexene (&)-3 is completely stable when treated with ZnC1, in CH2C12, but obviously, it is not stable when butynone is also present. Probably, the proton necessary for isomerisation (see also [ll]) originates from the complex between butynone and ZnC1,.