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Enantioselective Synthesis of Functionalised Decalones by Robinson Annulation of Substituted Cyclohexanones, Derived from R-(−)-Carvone

✍ Scribed by Ben J.M Jansen; Cindy C.J Hendrikx; Nikolai Masalov; Gerrit A Stork; Tommi M Meulemans; Fliur Z Macaev; Aede de Groot

Book ID: 108370770
Publisher: Elsevier Science
Year: 2000
Tongue: French
Weight: 489 KB
Volume: 56
Category: Article
ISSN: 0040-4020
DOI: 10.1016/s0040-4020(00)00110-1

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Copper (I) catalysed conjugate addition of methylmagnesium iodide to R-(-)-carvone and trapping the enolate as its trimethylsilyl enol ether, followed by a trityl perchlorate (TrCI04) catalysed Mukaiyama-aldol reaction, is an efficient method for the preparation of highly functionalised cyclohexanon