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Enantioselective Synthesis and Olfactory Evaluation of 13-Alkyl-Substituted α-Ionones

✍ Scribed by Marco Luparia; Paolo Boschetti; Francesca Piccinini; Alessio Porta; Giuseppe Zanoni; Giovanni Vidari

Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
279 KB
Volume
5
Category
Article
ISSN
1612-1872

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✍ Claudio Fuganti; Stefano Serra; Alessandro Zenoni 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 German ⚖ 100 KB

The synthesis of enantiomerically pure ()-and (À)-g-ionone 3 is reported. The first step in the synthesis is the diastereoisomeric enrichment of 4-nitrobenzoate derivatives of racemic g-ionol 12. The enantioselective lipase-mediated kinetic acetylation of g-ionol 13b afforded the acetate 14 and the