Rapid acquisition of 1H–13C and 1H–15N h
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Gary E. Martin; Chad E. Hadden; Albert N. Tackie; Maged M. H. Sharaf; Paul L. Sc
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Article
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1999
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John Wiley and Sons
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English
⚖ 132 KB
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The application of submicro inverse-detection gradient (SMIDG) NMR probe technology at 600 MHz is demonstrated for the rapid acquisition of both 1 H-13 C and 1 H-15 N heteronuclear chemical shift correlation data. Using a 750 µg (ca 1.5 µmol, MW 505) sample of the complex spirononacyclic alkaloid cr