Electrosynthesis and spectroscopic characterization of poly-para-phenylene films prepared by oxidation of benzene in liquid sulfur dioxide

Poly(3-chlorothiophene) films prepared b

Poly(3-chlorothiophene) films prepared by the direct electrochemical oxidation of 3-chlorothiophene in mixed electrolytes of boron trifluoride diethyl etherate and sulfuric acid

✍ Jingkun Xu; Gaoquan Shi; Fengen Chen; Fan Wang; Jiaxin Zhang; Xiaoyin Hong 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 215 KB

## Abstract 3‐Chlorothiophene (CT) was electrochemically polymerized in mixed electrolytes of a boron trifluoride diethyl etherate solution containing 0–20% (by volume) sulfuric acid. The oxidation potentials of the monomer in these media were measured to be only 1.06–1.31 V (vs Ag/AgCl). These val