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Electroreduction of β-chloropropiophenone: a study of stability of cis and trans isomers of 1,5-diphenyl-2,6-dioxa[3,3,0]bicyclooctane and on the logical reaction pathway

✍ Scribed by V.G. García; F. Cases; V. Montiel; E. San Fabián; A. Aldaz

Book ID
113257341
Publisher
Elsevier Science
Year
1991
Tongue
English
Weight
282 KB
Volume
231
Category
Article
ISSN
0166-1280

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✍ Ian Mc Ewen 📂 Article 📅 1993 🏛 Wiley (John Wiley & Sons) 🌐 English ⚖ 692 KB

The cyclic hexapeptide cycle[ -Pro'-Gly2-Glu3 (OBzl) -Pro4-Phe5-Leu6-] ( 1 ; OBzl: benzyl ester) was modeled and synthesized to be used as a chiral site for the separation of enantiomers. Total correlation spectroscopy and nuclear Ovehauser effect spectroscopy spectra of the peptide in CDCIB showed