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Electrooxidative Glycosylation Through C—S Bond Cleavage of 1-Arylthio-2,3-dideoxyglycosides. Synthesis of 2′,3′-Dideoxynucleosides.

✍ Scribed by Koichi Mitsudo; Takashi Kawaguchi; Seiji Miyahara; Wataru Matsuda; Manabu Kuroboshi; Hideo Tanaka

Publisher
John Wiley and Sons
Year
2006
Weight
28 KB
Volume
37
Category
Article
ISSN
0931-7597

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✍ Koichi Mitsudo; Wataru Matsuda; Seiji Miyahara; Hideo Tanaka 📂 Article 📅 2006 🏛 John Wiley and Sons ⚖ 26 KB 👁 1 views

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Synthesis of (R, S)-[2,3-13C2]-1-(1′-met
Synthesis of (R, S)-[2,3-13C2]-1-(1′-methyl-2′-pyrrolidinyl)propan-2-one; {(R, S)-[2′,3′-13C2]hygrine}
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2-Ethoxy-1-methyl-5-pymlidinone (1) was reacted with ethyl [3,4-'3C2]acetoacetate (2) in the presence of T i c 4 to give ethyl [3,4-13C2]-2-( 1'-methyl-5'oxo-2'-pyrrolidinyl)-3-oxobutanoate (3) in 85% yield. Decarboethoxylation of ethyl [3,4-13C2]-2-( l'-methyl-5'-oxo-2'-pyrrolidiny1)-3-oxobutanoate