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Electroorganic synthesis under solvent-free conditions. Highly regioselective anodic monofluorination of cyclic ethers, lactones, and a cyclic carbonate

✍ Scribed by Masaru Hasegawa; Hideki Ishii; Toshio Fuchigami

Publisher: Elsevier Science
Year: 2002
Tongue: French
Weight: 60 KB
Volume: 43
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(02)00047-3

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✦ Synopsis

Regioselective anodic fluorination of cyclic ethers, lactones, and a cyclic carbonate in Et 4 NF•nHF (n=4, 5) and Et 3 N•5HF without a solvent was successfully carried out to give the corresponding monofluorinated products in moderate yields. This is the first report of direct electrochemical fluorination of cyclic ethers, lactones, and a cyclic carbonate using anodic fluorination.

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