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Electronic and molecular structures of the octahedral Cp6M6A8, trigonal-bipyramidal Cp5M5A6, and tetrahedral Cp4M4A4 clusters

✍ Scribed by Bottomley, Frank.; Grein, Friedrich.

Book ID
127220476
Publisher
American Chemical Society
Year
1982
Tongue
English
Weight
994 KB
Volume
21
Category
Article
ISSN
0020-1669

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The reaction of [Cp\*MCl 4 ] (M Ο­ Nb, Ta; Cp\* Ο­ C 5 Me 5 ) with PH 2 R in toluene at room temperature gives the primary phosphine complexes [Cp\*MCl 4 (PH 2 R)] [Cp\* Ο­ C 5 Me 5 ; M Ο­ Nb: R Ο­ Bu t (1a), Ad (2a), Cy (3a), Ph (4a), 2,4,6-Me 3 C 6 H 2 (Mes) (5a); M Ο­ Ta: R Ο­ Bu t (1b), Ad (2b), Cy (3b