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Electrolytical reduction of maleinamide and fumaramide of 2-nitrobiphenyl-2′-amine at mercury electrodes

✍ Scribed by Jaromír Hlavatý; Jiří Volke; Osvald Manoušek

Publisher
Elsevier Science
Year
1979
Tongue
English
Weight
718 KB
Volume
24
Category
Article
ISSN
0013-4686

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✦ Synopsis

Aheaact -The role played by geometric isomerism in the intramolecular cychzation reaction initiated by the electrode reduction of makinamidc and fiunaramide of Z-nitrobiphenyl-2'-amine was studied at mercury electrodes. The cyclization reaction leading to the formation of benzo(c)cinnoline occurs with the former substance whereas only a reduction of the nitro group and of the C-C double bond could bc observed with the latter.

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Theoretical treatments for the kinetic parameters KS and a have been given by Delahay, Koutecky, Randles, Matsuda and Gellings. The analysis of irreversible polarographic waves a8 proposed by Matsuda and Gellings merits further discussion and application for calculating the kinetic parameters for a