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Electrolytic synthesis of nipecotic acid ethyl ester

✍ Scribed by M. Z. Muldakhmetov; A. M. Gazaliev; I. V. Kirilyus; S. D. Fazylov

Book ID
111461943
Publisher
SP MAIK Nauka/Interperiodica
Year
2007
Tongue
English
Weight
45 KB
Volume
80
Category
Article
ISSN
1070-4272

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## Abstract In a first step, Ξ”1‐trans‐octenoic‐3‐^14^C acid was prepared by a Grignard reaction with BaCO~3~‐^14^C and 1‐bromo‐pentane, followed by reduction of the obtained hexanoic‐1‐^14^C acid to hexanal‐1‐^14^C via the n‐hexanol‐1‐^14^C. The produced hexanal‐1‐^14^C, by condensing with malonic