Electrolytic reduction of carrier-free 188Re
β Scribed by Ekaterina Dadachova; Suzanne V. Smith; Saed Mirzadeh
- Publisher
- Elsevier Science
- Year
- 1996
- Tongue
- English
- Weight
- 295 KB
- Volume
- 47
- Category
- Article
- ISSN
- 0969-8043
No coin nor oath required. For personal study only.
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## Abstract Rheniumβ188βlabeled ReOCl~3~(PPh~3~)~2~ is an important reactive complex which can be prepared in > 95% yield by the reaction of perrhenate (^188^ReO~4~^β^) or perrhenic acid with triphenyl phosphine (PPh~3~) and HCl with subsequent extraction into CH~2~Cl~2~ or CHCl~3~. The yield is de