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Electrolytic partial fluorination of organic compounds. Part 50: Highly selective anodic mono- and difluorination of 4-phenylthiomethyl-1,3-dioxolan-2-one and its synthetic application

โœ Scribed by Katsutoshi Suzuki; Hideki Ishii; Toshio Fuchigami


Book ID
104230933
Publisher
Elsevier Science
Year
2001
Tongue
French
Weight
59 KB
Volume
42
Category
Article
ISSN
0040-4039

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Electrolytic partial fluorination of org
โœ Mohamed R Shaaban; Toshio Fuchigami ๐Ÿ“‚ Article ๐Ÿ“… 2002 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 75 KB

Constant potential anodic oxidation of s-triazolo [3,4-b][1,3,4]thiadiazine derivatives in DME containing Et 4 NFโ€ข4HF using an undivided cell provided the corresponding 7-monofluorinated products predominantly in good to moderate yields. 7,7-Difluorination was also anodically achieved.