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Electrochemical synthesis of a pseudo-two-dimensional polytelluride containing Te2−12 anions: structure of [(C2H5)4N]2Te12

✍ Scribed by Christopher J. Warren; Robert C. Haushalter; Andrew B. Bocarsly

Book ID
116160765
Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
844 KB
Volume
233
Category
Article
ISSN
0925-8388

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Red crystals of [H 3 O ´(dibenzo-18-crown-6)][Te 2 Br 9 ] (1) were isolated from a solution of TeBr 4 and dibenzo-18crown-6 in CH 3 CN containing a small amount of hydrobromic acid. The compound crystallizes in the triclinic space group P 1 with the cell dimensions a = 9.010(2), b = 13.403(3), c = 1