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Electrochemical studies of copper(II) 2-acetylpyridine4N-dialkylthiosemicarbazones. Relation to their spectral, magnetic, and biological properties

✍ Scribed by Avinash S. Kumbhar; Subhash B. Padhye; Douglas X. West; Anthony E. Liberta

Publisher
Springer
Year
1991
Tongue
English
Weight
397 KB
Volume
16
Category
Article
ISSN
0340-4285

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The anion (loss of 3N hydrogen) of 2-acetylpyridine 4N-methylthiosemicarbazone coordinates in a planar conformation to copper(II) through the pyridyl nitrogen, azomethine nitrogen and thiolato sulphur atoms. The fourth coordination site is occupied by a bromo ligand and the complex is mononuclear an

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Copper(II) complexes of a large number of 2-acetylpyridine 4N-alkylthiosemicarbazones were prepared and characterized. I.r., electronic and e.s.r, spectra of the complexes, as well as 1H and ~3C n.m.r, spectra of the thiosemicarbazones, were obtained. Both the thiosemicarbazones and their complexes