Electrochemical Crystallization of Cuprous Oxide with Systematic Shape Evolution

✍ Scribed by M. J. Siegfried; K.-S. Choi

• Publisher: John Wiley and Sons
• Year: 2004
• Tongue: English
• Weight: 332 KB
• Volume: 16
• Category: Article
• ISSN: 0935-9648
• DOI: 10.1002/adma.200400177

✦ Synopsis

typically 3±5 nm in size, were used for growing the nanostructures. After the evacuation process was completed, the temperature of the system was elevated to 750 C at a rate of 20 C min ±1 and the pressure was maintained at 30 kPa. Nitrogen was sent through the system at a rate of 50 mL min ±1 to act as a carrier gas to transport the sublimated vapor to cooler regions within the tube furnace for deposition. The asproduced materials were analyzed by scanning electron microscopy and high-resolution transmission electron microscopy.