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Electrochemical construction of the diaryl ethers: a synthetic approach to o-methylthalibrine

✍ Scribed by Yu Naito; Takamasa Tanabe; Yuki Kawabata; Yuichi Ishikawa; Shigeru Nishiyama

Book ID: 104098072
Publisher: Elsevier Science
Year: 2010
Tongue: French
Weight: 438 KB
Volume: 51
Category: Article
ISSN: 0040-4039
DOI: 10.1016/j.tetlet.2010.07.037

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✦ Synopsis

Electrochemical dimerization of halogenated p-hydroxyphenylacetic acid derivatives followed by Zn reduction provided the corresponding diaryl ethers. Manipulation of the reduction step using several procedures increased its efficiency, which enabled the construction of o-methylthalibrine, an isoquinolineclass alkaloid.

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