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Ein Komplex mit Arsen- und Carbamoyl-Brücke: Darstellung und Struktur von Fe2(CO)6[μ-As(CH3)2][μ-OCN(CH3)2]

✍ Scribed by Keller, Egbert ;Trenkle, Armin ;Vahrenkamp, Heinrich


Publisher
Wiley (John Wiley & Sons)
Year
1977
Tongue
English
Weight
400 KB
Volume
110
Category
Article
ISSN
0009-2940

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✍ H. Ackermann; R. Leo; W. Massa; K. Dehnicke 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 German ⚖ 76 KB 👁 1 views

The title compound was prepared from cobalt(II) acetate with Me 3 SiNPEt 3 at 180 °C and subsequent crystallization from diethylether to give blue, moisture sensitive single crystals, which were characterized by a crystal structure determination. Space group P2 1 /n, Z = 2, lattice dimensions at ±80