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Efficient Synthesis of 2,8-Diphosphatricyclo[5.3.1.12,6]dodeca-3,5,9-triene 2,8-Dioxides.

✍ Scribed by Janos Kovacs; Timea Imre; Krisztina Ludanyi; Laszlo Toke; Gyoergy Keglevich

Publisher
John Wiley and Sons
Year
2004
Weight
133 KB
Volume
35
Category
Article
ISSN
0931-7597

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## Abstract Trimerization of butadiene in the presence of Ni(0) affords (1__E__,5__E__,9__E__)‐cyclododeca‐1,5,9‐triene **1** (__ttt__‐CDT), (1__E__,5__E__,9__Z__)‐cyclododeca‐1,5,9‐triene **2** (__ttc__‐CDT), and other isomers/oligomers. After optimization of reaction conditions, [^14^C~6~‐3,4,7,8