The rapid and efficient synthesis of d(TTTATT) and d(CATGAGGAAGT) on glass beads of controlled pore size using N-acylated 5'-O-trityldeoxynucleoside-3'-(2-chloro)-phenyl phosphates as phosphate components, capping with acetic anhydride, detritylation with ZnBr2 and 1-(mesitylene-2-sulphonyl)-3-nitro
β¦ LIBER β¦
Efficient syntheses of an oligonucleotide on a cellulose acetate derivative as a novel polymer-support using phosphotriester approach
β Scribed by Kazuo Kamaike; Yoshihiro Hasegawa; Yoshiharu Ishido
- Book ID
- 108381607
- Publisher
- Elsevier Science
- Year
- 1988
- Tongue
- French
- Weight
- 276 KB
- Volume
- 29
- Category
- Article
- ISSN
- 0040-4039
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A useful and novel application of polymer-supported IBX for the chemoselective and regioselective oxidation of phenolic compounds has been described. Hydroxytyrosol and carboxymethylated hydroxytyrosol have been prepared in good conversions and yields under green chemistry conditions in the presence