𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Efficient solvent-free synthesis of thiazolidin-4-ones from phenylhydrazine and 2,4-dinitrophenylhydrazine

✍ Scribed by Patrícia D. Neuenfeldt; Bruna B. Drawanz; Geonir M. Siqueira; Claudia R.B. Gomes; Solange M.S.V. Wardell; Alex F.C. Flores; Wilson Cunico

Book ID
104097714
Publisher
Elsevier Science
Year
2010
Tongue
French
Weight
294 KB
Volume
51
Category
Article
ISSN
0040-4039

No coin nor oath required. For personal study only.

✦ Synopsis

An efficient solvent-free synthesis of thiazolidinones from reaction of mercaptoacetic acid, aldehydes (benzaldehyde and valeraldehyde) or ketones (cyclopentanone and cyclohexanone), and hydrazines (phenylhydrazine and 2,4-dinitrophenylhydrazine) is reported. The compounds were generally characterized by spectroscopic techniques and specifically for 2-cyclohexanyl-3-(N-phenyl)-1,3-thiazolidin-4-one by X-ray crystallography.

📜 SIMILAR VOLUMES

Microwave Induced Synthesis of the Thiaz
Microwave Induced Synthesis of the Thiazolidine-2,4-dione Motif and the Efficient Solvent Free-Solid Phase Parallel Syntheses of 5-Benzylidene-thiazolidine-2,4-dione and 5-Benzylidene-2-thioxo-thiazolidine-4-one Compounds.
✍ B. R. Prashantha Kumar; M. D. Karvekar; L. Adhikary; M. J. Nanjan; B. Suresh 📂 Article 📅 2006 🏛 John Wiley and Sons ⚖ 17 KB 👁 2 views

## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract, please click on HTML or PDF.

Microwave induced synthesis of the thiaz
Microwave induced synthesis of the thiazolidine-2,4-dione motif and the efficient solvent free-solid phase parallel syntheses of 5-benzylidene-thiazolidine-2,4-dione and 5-benzylidene-2-thioxo-thiazolidine-4-one compounds
✍ B. R. Prashantha Kumar; M. J. Nanjan; B. Suresh; M. D. Karvekar; L. Adhikary 📂 Article 📅 2006 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 111 KB

## Abstract magnified image Novel microwave induced method for the synthesis of thiazolidine‐2,4‐dione motif under solvent phase conditions is developed. Further we report an efficient, microwave assisted method for the parallel syntheses of biologically important 5‐benzylidene‐thiazolidine‐2,4‐di