Efficient Preparation of 4-Iodofuran-2(5H)-ones by Iodolactonisation of 2,3-Allenoates with I2
✍ Scribed by Chunling Fu; Shengming Ma
- Publisher
- John Wiley and Sons
- Year
- 2005
- Tongue
- English
- Weight
- 83 KB
- Volume
- 2005
- Category
- Article
- ISSN
- 1434-193X
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## Abstract A new synthetic route to 6‐substituted‐imidazo[4,5‐__c__]pyridin‐2‐ons from 4‐aminopyridine has been investigated. 4‐Aminopyridine protected as alkyl carbamates were nitrated with dinitrogen pentoxide to the corresponding methyl, __i__‐propyl and __t__‐butyl 3‐nitropyridin‐4‐yl carbamat
## Abstract magnified image A new method for the synthesis of substituted 5‐(2‐hydroxyethyl)‐2‐phenylimino‐1,3‐thiazolidin‐4‐ones and 5‐(2‐hydroxyethyl)‐2‐phenylamino‐4,5‐dihydro‐1,3‐thiazol‐4‐ones is described, starting from phenylthioureas and 3‐bromotetrahydrofuran‐2‐one. The reaction proceeds