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Efficient Oxidation of Sulfides to Sulfoxides and of Thiols to Disulfides with Aqueous HIO3

✍ Scribed by F. Shirini; M. A. Zolfigol; M. M. Lakouraj; M. R. Azadbar

Book ID
110318941
Publisher
SP MAIK Nauka/Interperiodica
Year
2001
Tongue
English
Weight
19 KB
Volume
37
Category
Article
ISSN
1070-4280

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ChemInform Abstract: Efficient Oxidation
ChemInform Abstract: Efficient Oxidation of Sulfides to Sulfoxides and of Thiols to Disulfides with Aqueous HIO3.
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An efficient asymmetric oxidation of sul
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The Sharpless reagent (Ti(OiPr)4 t 1 mol eq. diethyl tartrate (DET) t 2 J-BuOOH) modified by addition of one mol eq. H20 gives a new homogeneous reagent which cleanly oxidizes sulfidesinto sulfoxides in dichloromethane. The best results were obtained for the stoichiometry Ti/DET/ H20/J-BuOOH = 1:2:1