Effects of restricted molecular motion on the high-resolution solid-state 13C CP MAS NMR spectrum of the nitrile group of the stearonitrile-urea inclusion complex

High-resolution 13C NMR study of free an

High-resolution 13C NMR study of free and metal-complexed ionophores in the solid state: Conformation and dynamics of the macrocyclic ring and the effect of intermolecular short contact of methyl groups on spin–lattice relaxation times and displacements of chemical shifts

✍ Hazime Saitô; Ryoko Tabeta; Motoko Yokoi 📂 Article 📅 1988 🏛 John Wiley and Sons 🌐 English ⚖ 819 KB

High-resolution 13C NMR spectra of 15 samples of uncomplexed and metalcomplexed tetranactin and nonactin were recorded in the solid state, revealing characteristic displacements of peaks due to complex formation and the effect of crystalline packing on the 13C chemical shifts and spidattice relaxati