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Effect of the evaporation of various solvents upon the stability of corticosterone-1,2-3H and corticosterone-4-14C

✍ Scribed by Arthur I. Frankel; Andrem V. Nalbandov

Book ID
118977285
Publisher
Elsevier Science
Year
1966
Tongue
English
Weight
772 KB
Volume
8
Category
Article
ISSN
0039-128X

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## Abstract Reaction of isonicotinic [^14^C] acid hydrazide (**1**) with the Zinke salt (**2**) afforded N‐(4‐pyridyl [^14^C] carbonylimino)pyridinium ylide (**3**) in 81% chemical yield. Sodium borohydride reduction of **3** gave N‐(4‐pyridyl [^14^C] carbonylamino) βˆ’1,2,3,6‐tetrahydropyridine (**4