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Effect of Oxygen Vacancy on Phase Transition and Photoluminescence Properties of Nanocrystalline Zirconia Synthesized by the One-Pot Reaction

✍ Scribed by Cong, Yan; Li, Bin; Yue, Shumei; Fan, Di; Wang, Xiao-jun


Book ID
118273894
Publisher
American Chemical Society
Year
2009
Tongue
English
Weight
254 KB
Volume
113
Category
Article
ISSN
1932-7447

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Two powdered batches of undoped zirconia, prepared by spray pyrolysis and characterized by 6.9 and 13.2 nm average crystallite size were annealed for di4erent temperatures and for di4erent times. The tetragonal+monoclinic phase transformation was monitored by Raman spectroscopy and X-ray di4raction.