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Effect of Al addition on the synthesis of Ti3SiC2 bulk material by pulse discharge sintering process

✍ Scribed by Songlan Yang; ZhengMing Sun; Qiaoqin Yang; Hitoshi Hashimoto

Publisher: Elsevier Science
Year: 2007
Tongue: English
Weight: 524 KB
Volume: 27
Category: Article
ISSN: 0955-2219
DOI: 10.1016/j.jeurceramsoc.2007.03.038

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✦ Synopsis

Ti 3 SiC 2 bulk materials were synthesized from the starting powders of 1Ti/1Si/2TiC-xAl and 3Ti/1SiC/1C-xAl (molar ratios, x ranges from 0.05 to 0.15) at temperatures between 1100 and 1400 • C for 15 min by pulse discharge sintering technique. X-ray diffraction and scanning electron microscopy were used to characterize the synthesized materials. It was found that the addition of Al decreases the content of TiC in the sintered samples and expands the optimal temperature range for the synthesis of Ti 3 SiC 2 bulk materials. By addition of Al, Ti 3 SiC 2 bulk materials of high phase-purity have been synthesized at 1100 and 1200 • C from 1Ti/1Si/2TiC and 3Ti/1SiC/1C starting powders, respectively.

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