(E)-2-Methoxy-N′-[4-methoxy-3-(4-methylphenylsulfonyloxy)benzylidene]benzohydrazide ethanol solvate hemihydrate
✍ Scribed by Chen, Xin ;Yu, Ming
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 169 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
In the title compound, C 21 H 18 N 4 O 5 , the central vanillin group makes dihedral angles of 8.76 (13) and 62.38 (6) with its attached pyridine and nitrobenzene rings, respectively. The crystal packing is stabilized by N-HÁ Á ÁN hydrogen bonds and C-HÁ Á ÁO interactions, leading to an infinite net
Single-crystal X-ray study T = 294 K Mean (C-C) = 0.005 A R factor = 0.049 wR factor = 0.131 Data-to-parameter ratio = 12.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C 21 H 19 N 3 O 6 S, the vanillin group makes dihedral angles of 56.00 (7) and 7.22 (8) with the 4-methylbenzene ring and the nitrophenylhydrazine ring, respectively. The crystal packing is stabilized by intermolecular N-HÁ Á ÁO hydrogen bonds and weak, non-classical intermole
The title compound, C 21 H 19 N 3 O 6 S, crystallizes with two molecules in the asymmetric unit. The conformations of these non-planar molecules are similar. Intermolecular N-HÁ Á ÁO and C-HÁ Á ÁO hydrogen bonds help to consolidate the crystal structure.