The synthesis of t h e title canpound (7) is described. [2-14C] cytosine (I) is treated with an aqueous mixture of sodium bisulfite and sodium sulfate at 8OoC for 30 rnin. The resulting solid is then treated with aqueous sodiun hydroxide and passed through a cation exchange colunn, producing [ Z-14C
(E)-1-(2′-Deoxy-β-d-ribofuranosyl)-2,4-difluoro-5-(2-iodovinyl)benzene
✍ Scribed by Mark, Brian L. ;Parrish, Jonathan C. ;Wang, Zhi-Xian ;Wiebe, Leonard I. ;Knaus, Edward E. ;James, Michael N. G.
- Book ID
- 119980717
- Publisher
- International Union of Crystallography
- Year
- 2001
- Tongue
- English
- Weight
- 91 KB
- Volume
- 57
- Category
- Article
- ISSN
- 0108-2701
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 297 K Mean '(C±C) = 0.013 A Ê R factor = 0.045 wR factor = 0.125 Data-to-parameter ratio = 14.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 290 K Mean '(C±C) = 0.007 A Ê R factor = 0.038 wR factor = 0.094 Data-to-parameter ratio = 15.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.