Dyotropic Rearrangements, a New Class of
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Dr. Manfred T. Reetz
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Article
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1972
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John Wiley and Sons
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English
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vacuum, (2) crystallizes out (m. p. 70-72 "C after recrystallization from ethyl acetate/petroleum ether) ; yield ca. A mixture of (2) (249 g, 1 mol), trimethylchlorosilane (108 g, 1 mol), and triethylamine (101 g, 1 mol) in toluene (1.2 1) is heated to boiling for 2 h, allowed to cool and then filt