## Two-dimensional high-resolution solid-state NMR has been used to study 13C-enriched wood. Wood is a complex material containing three major polymers: cellulose, hemicelluloses and lignin. The use of an enriched '3C-compound allows the observation of intra-molecular spin-diffusion driven by dipo
Dynamics of 9-Hydroxyphenalenone Studied by One-Dimensional Solid-State Spin Exchange NMR
β Scribed by Kuwahara, Daisuke; Koyano, Hiroyuki; Manaka, Taisuke; Nakamura, Hideaki; Mochida, Tomoyuki; Sugawara, Tadashi
- Book ID
- 126774950
- Publisher
- American Chemical Society
- Year
- 2006
- Tongue
- English
- Weight
- 82 KB
- Volume
- 110
- Category
- Article
- ISSN
- 1089-5639
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The locus of the photodimerization reaction of 9-methylanthracene in the crystal was examined by high-resolution solid-state 13C NMR techniques. Examination of the 13C spectra of the products showed that only the trans dimer is formed by the solid state photodimerization, while both trans and cis di
Molecular motions of polycrystalline cellobiose have been investigated by measuring proton spin-lattice relaxation times, T1 and T1rho, and the second moment, M2, in both protonated and D2O exchanged forms over the temperature range 120-380 K. T1 relaxation is dominated by the motions of hydroxyl gr