Dynamic polarization and relaxation of protons in 1,6-hexanediol and 1,8-octanediol: A feasibility study for a frozen spin polarized target

A variable-temperature 13C cross-polariz

A variable-temperature 13C cross-polarization magic angle spinning NMR study of some unusual dynamic and phase properties of (±)-3,4-di-O-acetyl-1,2,5,6-tetra-O-benzyl-myo-inositol, ‘jumping crystals’

✍ Jamila Fattah; J. Mark Twyman; Christopher M. Dobson 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 English ⚖ 598 KB

## Abstract Variable‐temperature ^13^C CP/MAS NMR experiments were carried out on crystalline (±)‐3,4‐di‐__O__‐acetyl‐1,2,5,6‐tetra‐__O__‐benzyl‐__myo__‐inositol. Three distinct phases can be distinguished from their NMR characteristics, each stable over a well defined temperature range, in accord