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Durable press finishing of cotton with polycarboxylic acids. I. Preparation of thiosuccinyl-s-triazine

✍ Scribed by D. M. Lewis; B. Voncina

Publisher: John Wiley and Sons
Year: 1997
Tongue: English
Weight: 223 KB
Volume: 66
Category: Article
ISSN: 0021-8995
DOI: 10.1002/(sici)1097-4628(19971121)66:8<1465::aid-app7>3.0.co;2-c

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✦ Synopsis

The preparation of an alternative polycarboxylic acid to replace the most promising, but expensive, crosslinking reagent 1,2,3,4-butanetetracarboxylic acid (BTCA) is reported. The reaction of mercaptosuccinic acid with 2,4,6-trichloro-s-triazine (cyanuric chloride) gave a dithiosuccinyl derivative. The preparation reaction was followed using horizontal ATR infrared spectroscopy and capillary electrophoresis. The final product was characterized by FTIR, capillary electrophoresis, and 1 H-NMR.

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