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Dreikomponentenreaktionen. XIV. 2-Imidazoline und 1,2,4-Triazole durch Ringschlußreaktionen von N-(2-Chlor-alkyl)imidchloriden mit Hydrazin und Hydrazonen

✍ Scribed by Dr. R. Neumann; Prof. Dr. J. Beger


Publisher
John Wiley and Sons
Year
1982
Tongue
English
Weight
379 KB
Volume
324
Category
Article
ISSN
1615-4150

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✦ Synopsis


Three Component Reactions. XIV. 2‐Imidazolines and 1,2,4‐Triazoles by Ring Closure Reactions of N‐(2‐Chloro‐alkyl)imidchlorides with Hydrazine and Hydrazones

N‐(2‐Chloro‐alkyl)benzimidchlorides (1a and 1b) give with hydrazine in dependence on the reaction medium 1,1′‐bis(2‐imidazolines) (4), 1‐benzamido‐2‐imidazolines (5) or 1,2,4‐triazoles (6 and 7) and also N‐(2‐chloro‐alkyl)benzamides (8). From imidchlorides (1a–c) and hydrazones Schiff bases (10) of 1‐amino‐2‐imidazolines are obtained. They are not cleavable into free 1‐amino‐2‐imidazolines. magnified image