A simplified and effective phase separator for use in flow systems is described. The sample, 300 l, is introduced into an aqueous stream (flow injection). The aqueous phase, containing the sample plugs, is divided into small segments by an organic phase using a commercial T-connector. Separation of
Double-membrane phase separator for liquid-liquid extraction in flow-injection analysis
✍ Scribed by Tadao Sakai; Yong Soon Chung; Noriko Ohno; Shoji Motomizu
- Publisher
- Elsevier Science
- Year
- 1993
- Tongue
- English
- Weight
- 392 KB
- Volume
- 276
- Category
- Article
- ISSN
- 0003-2670
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✦ Synopsis
A double-membrane phase separator for liquid-liquid extraction in flow-injection analysis was designed and its usefulness was examined in order to achieve smooth, long-term and efficient phase separation with good reproducibility. The construction and performance of the flow-injection system using the phase separator were illustrated by the extraction of berberine-perchlorate ion associates.
📜 SIMILAR VOLUMES
A sensitive and rapid determination of berberine was carried out by flow-injection analysis. Berberine was successfully extracted in the presence of sodium perchlorate. The calibration graph was linear over the range 4 X 10d9-1 X 1O-6 mol dm-". The sample throughput was 42 h-l.
## Abstract Hollow fiber‐based liquid–liquid–liquid microextraction (HF‐LLLME) followed by flow injection analysis and diode array detection (FIA‐DAD) was applied as a simple and sensitive quantitative method for the determination of phenazopyridine in urine and plasma samples. Flow injection syste