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DNA-ligand interaction detected by proton selective and non-selective spin-lattice relaxation rate analysis

✍ Scribed by Claudia Bonechi; Alessandro Donati; Maria Pia Picchi; Claudio Rossi; Enzo Tiezzi


Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
423 KB
Volume
115
Category
Article
ISSN
0927-7757

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✦ Synopsis


In this paper, a method based on NMR measurements for studying the ability of ligands to interact with macromolecule surfaces is proposed. It is based on temperature-dependent NMR proton selective and non-selective spin lattice relaxation rate experiments and assumes fast chemical exchange conditions of the ligand between free and bound states. The results obtained appear able to identify DNA-psoralen complex formation. The use of this melhodology for monitoring non-covalent interaction of ligands and bipolymers is suggested.